Analytical Electrochemistry / Edition 3

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Overview

Providing a sound understanding of the fundamentals of electrode reactions and of the principles of electrochemical methods with a focus on the potential for solving real-life analytical problems this Third Edition has been thoroughly revised and updated to cover the latest developments in electroanalytical chemistry. This comprehensive reference includes recent advances in methodologies, sensors, detectors, and microchips, and establishes a balance between voltammetric and potentiometric techniques.

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Editorial Reviews

From the Publisher
"Anyone at any level wanting to get involved in electrochemical experimentation should benefit from access to this book." (CHOICE, October 2006)
Journal of Chemical Education
...this book shines as a self-consistent introduction to the techniques it claims to treat...fills an important niche in the library holdings of any institution of higher learning...those who...frequently deal with research involving the application of electroanalytical methods will likely find themselves reaching for it often.
SciTech Book News
Offers clear, reader-friendly explanations of fundamental principles of electrochemical processes as well as insight...
Choice
...useful for a novice hoping to learn whether electrochemistry might be helpful in a particular case...useful for upper-division...or graduate students contemplating electrochemical research...
Booknews
Offers clear, reader-friendly explanations of fundamental principles of electrochemical processes as well as insight into the potential of electroanalysis for problem solving in a range of fields, from clinical diagnostics to environmental science. Examines aspects of electrode reactions, discusses high-resolution surface characterization, and overviews finite-current controlled-potential techniques. Describes electrochemical instrumentation and electrode materials, deals with principles of potentiometric measurements, and examines chemical sensors. Includes b&w photos of equipment. For advanced undergraduates and graduate students. This edition expands theoretical discussion and covers the latest advances in the field through 1999. Wang teaches chemistry at New Mexico State University. Annotation c. Book News, Inc., Portland, OR booknews.com
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Product Details

  • ISBN-13: 9780471678793
  • Publisher: Wiley
  • Publication date: 5/5/2006
  • Edition description: REV
  • Edition number: 3
  • Pages: 272
  • Product dimensions: 6.48 (w) x 9.27 (h) x 0.71 (d)

Meet the Author

JOSEPH WANG, PHD, is Director of the Center for Bioelectronics and Biosensors at the Biodesign Institute and Professor in the Departments of Chemical & Materials Engineering and Chemistry & Biochemistry at Arizona State University. Dr. Wang has authored six books and more than 680 research papers. He holds fifteen patents and is the recipient of the American Chemical Society's Award in Chemical Instrumentation and the Heyrovsky Medal. He was ranked the "Most Cited Electrochemist in the World" in 1995, and was ranked number five on the ISI list of "Most Cited Researchers in Chemistry" for the period 1995 to 2005.

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Table of Contents

Preface.

Abbreviations and Symbols.

1. Fundamental Concepts.

1.1 Why Electroanalysis?

1.2 Faradaic Processes.

1.2.1 Mass-Transport-Controlled Reactions.

1.2.1.1 Potential-Step Experiment.

1.2.1.2 Potential-Sweep Experiments.

1.2.2 Reactions Controlled by the Rate of Electron Transfer.

1.2.2.1 Activated Complex Theory.

1.3 Electrical Double Layer.

1.4 Electrocapillary Effect.

1.5 Supplementary Reading.

Problems.

References.

2. Study of Electrode Reactions and InterfacialProperties.

2.1 Cyclic Voltammetry.

2.1.1 Data Interpretation.

2.1.1.1 Reversible Systems.

2.1.1.2 Irreversible and Quasi-reversible Systems.

2.1.2 Study of Reaction Mechanisms.

2.1.3 Study of Adsorption Processes.

2.1.4 Quantitative Applications.

2.2 Spectroelectrochemistry.

2.2.1 Experimental Arrangement.

2.2.2 Principles and Applications.

2.2.3 Electrochemiluminescence.

2.2.4 Optical Probing of Electrode–SolutionInterfaces.

2.3 Scanning Probe Microscopy.

2.3.1 Scanning Tunneling Microscopy.

2.3.2 Atomic Force Microscopy.

2.3.3 Scanning Electrochemical Microscopy.

2.4 Electrochemical Quartz Crystal Microbalance.

2.5 Impedance Spectroscopy.

Examples.

Problems.

References.

3. Controlled-Potential Techniques.

3.1 Chronoamperometry.

3.2 Polarography.

3.3 Pulse Voltammetry.

3.3.1 Normal-Pulse Voltammetry.

3.3.2 Differential-Pulse Voltammetry.

3.3.3 Square-Wave Voltammetry.

3.3.4 Staircase Voltammetry.

3.4 AC Voltammetry.

3.5 Stripping Analysis.

3.5.1 Anodic Stripping Voltammetry.

3.5.2 Potentiometric Stripping Analysis.

3.5.3 Adsorptive Stripping Voltammetry and Potentiometry.

3.5.4 Cathodic Stripping Voltammetry.

3.5.5 Abrasive Stripping Voltammetry.

3.5.6 Applications.

3.6 Flow Analysis.

3.6.1 Principles.

3.6.2 Cell Design.

3.6.3 Mass Transport and Current Response.

3.6.4 Detection Modes.

Examples.

Problems.

References.

4. Practical Considerations.

4.1 Electrochemical Cells.

4.2 Solvents and Supporting Electrolytes.

4.3 Oxygen Removal.

4.4 Instrumentation.

4.5 Working Electrodes.

4.5.1 Mercury Electrodes.

4.5.2 Solid Electrodes.

4.5.2.1 Rotating Disk and Rotating Ring Disk Electrodes.

4.5.2.2 Carbon Electrodes.

4.5.2.2.1 Glassy Carbon Electrodes.

4.5.2.2.2 Carbon Paste Electrodes.

4.5.2.2.3 Carbon Fiber Electrodes.

4.5.2.2.4 Diamond Electrodes.

4.5.2.3 Metal Electrodes.

4.5.3 Chemically Modified Electrodes.

4.5.3.1 Self-Assembled Monolayers.

4.5.3.2 Carbon-Nanotube-Modified Electrodes.

4.5.3.3 Sol-gel Encapsulation of Reactive Species.

4.5.3.4 Electrocatalytically Modified Electrodes.

4.5.3.5 Preconcentrating Electrodes.

4.5.3.6 Permselective Coatings.

4.5.3.7 Conducting Polymers.

4.5.4 Microelectrodes.

4.5.4.1 Diffusion at Microelectrodes.

4.5.4.2 Microelectrode Configurations.

4.5.4.3 Composite Electrodes.

Examples.

Problems.

References.

5. Potentiometry.

5.1 Principles of Potentiometric Measurements.

5.2 Ion-Selective Electrodes.

5.2.1 Glass Electrodes.

5.2.1.1 pH Electrodes.

5.2.1.2 Glass Electrodes for Other Cations.

5.2.2 Liquid Membrane Electrodes.

5.2.2.1 Ion Exchanger Electrodes.

5.2.2.2 Neutral Carrier Electrodes.

5.2.3 Solid-State Electrodes.

5.2.4 Coated-Wire Electrodes and Solid-State Electrodes Withoutan Internal Filling Solution.

5.3 On-line, On-site, and In Vivo PotentiometricMeasurements.

Examples.

Problems.

References.

6. Electrochemical Sensors.

6.1 Electrochemical Biosensors.

6.1.1 Enzyme-Based Electrodes.

6.1.1.1 Practical and Theoretical Considerations.

6.1.1.2 Enzyme Electrodes of Analytical Significance.

6.1.1.2.1 Glucose Sensors.

6.1.1.2.2 Ethanol Electrodes.

6.1.1.2.3 Urea Electrodes.

6.1.1.2.4 Toxin (Enzyme Inhibition) Biosensors.

6.1.1.3 Tissue and Bacteria Electrodes.

6.1.2 Affinity Biosensors.

6.1.2.1 Immunosensors.

6.1.2.2 DNA Hybridization Biosensors.

6.1.2.2.1 Background and Principles.

6.1.2.2.2 Electrical Transduction of DNA Hybridization.

6.1.2.2.3 Other Electrochemical DNA Biosensors.

6.1.2.3 Receptor-Based Sensors.

6.1.2.4 Electrochemical Sensors Based on Molecularly ImprintedPolymers.

6.2 Gas Sensors.

6.2.1 Carbon Dioxide Sensors.

6.2.2 Oxygen Electrodes.

6.3 Solid-State Devices.

6.3.1 Ion-Selective Field Effect Transistors.

6.3.2 Microfabrication of Solid-State Sensor Assemblies.

6.3.3 Microfabrication Techniques.

6.3.4 Micromachined Analytical Microsystems.

6.4 Sensor Arrays.

Examples.

Problems.

References.

Index.

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