Annual Reports on NMR Spectroscopy

Annual Reports on NMR Spectroscopy

by Graham A. Webb
     
 

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ISBN-10: 0125054513

ISBN-13: 9780125054515

Pub. Date: 12/18/2003

Publisher: Elsevier Science

Over recent years, no other technique has grown to such importance as that of NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a means for the specialist and

Overview

Over recent years, no other technique has grown to such importance as that of NMR spectroscopy. It is used in all branches of science where precise structural determination is required and where the nature of interactions and reactions in solution is being studied. Annual Reports on NMR Spectroscopy has established itself as a means for the specialist and non-specialist alike to become familiar with new applications of the technique in all branches of chemistry, including biochemistry and pharmaceutics.Once again, the Annual Reports on NMR Spectroscopy represents the best work in the field in both applied and theoretical NMR spectroscopy. The high caliber reports in Volume 41 show the wide biological and physical applications that benefit from this analytical technique. <%END%>

Product Details

ISBN-13:
9780125054515
Publisher:
Elsevier Science
Publication date:
12/18/2003
Series:
Annual Reports on NMR Spectroscopy Series
Pages:
312
Product dimensions:
0.75(w) x 6.14(h) x 9.21(d)

Table of Contents


Contributors     vii
Preface     ix
Structure and Membrane Interactions of Antimicrobial Peptides as Viewed by Solid-State NMR Spectroscopy   Marise Ouellet   Michele Auger     1
Introduction     2
Study of Antimicrobial Peptides in Membranes     3
Effects of Antimicrobial Peptides on Model Lipid Membranes     15
Conclusions     19
References     19
Chemical Exchange   Alex D. Bain     23
Introduction     23
Overview, Trends and Opinions     25
Theory     27
Methodology     32
Applications     35
Conclusions and Acknowledgments     43
References     44
Rhodium-103 NMR   Laurence Carlton     49
Introduction     50
Acquisition of Data     51
Calibration of Spectra     52
Factors Underlying the Chemical Shift     54
Influence of Temperature on the Chemical Shift     57
Influence of Solvent on the Chemical Shift     58
Other Influences on the Chemical Shift     61
Correlation of [delta]([superscript 103]Rh) with Chemical and Structural Parameters     65
Parahydrogen-Induced Polarisation (PHIP)     76
High-Pressure Studies     78
Solid-State Studies     78
Clusters     80
Calculated Chemical Shifts     82
Spin Coupling Constants     84
Relaxation Times     87
Conclusion     88
Abbreviations     88
Acknowledgements     90
Layout of Tables     90
References     167
The Indirect Detection of Metal Nuclei by Correlation Spectroscopy (HSQC and HMQC)   Jonathan A. Iggo   Jianke Liu   Gillian Overend     179
Introduction     180
2D NMR Spectroscopy     186
Spin Systems     200
Review of Recent Reports of the Indirect Detection of Metal Nuclei     211
Conclusions     255
Abbreviations     255
Acknowledgements     257
References     257
Subject Index     263

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