Capillary Electrochromatography and Pressurized Flow Capillary Electrochromatography: An Introduction

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Covers the theory, instrumentation, and specific uses and applications of capillary electrochromatography (CEC) and pressurized flow capillary electrochromatography (PEC). Discusses advantages and limitations of CEC/PEC compared with more conventional modes of separation and explains method development and optimization.

Introducing the fundamentals and literature to those first approaching applications in CEC/PEC, the book will serve as a ...
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Overview

Covers the theory, instrumentation, and specific uses and applications of capillary electrochromatography (CEC) and pressurized flow capillary electrochromatography (PEC). Discusses advantages and limitations of CEC/PEC compared with more conventional modes of separation and explains method development and optimization.

Introducing the fundamentals and literature to those first approaching applications in CEC/PEC, the book will serve as a valuable guide for analytical chemists and biochemists, molecular biologists, immunologists, pharmaceutical scientists, and environmental and industrial chemists.
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Product Details

  • ISBN-13: 9780966428629
  • Publisher: HNB Publishing
  • Publication date: 7/1/2000
  • Pages: 240

Table of Contents

TABLE OF CONTENTS: TOC:

1. Introduction
1.1 Some definitions and concepts
1.2 Capillary electrochromatography: the best of both worlds
1.3 Reproducibility
1.4 Selection of operating mode
1.5 Pressure-assisted CEC
1.6 Advantages of CEC
1.7 Limitations of CEC
Appendix: Symbols and units used in CEC
References

2. Capillary Column Technology
2.1 Packed Capillaries
2.2 Surface chemistry on particles
2.3 Techniques for packing capillaries
2.4 Packing protocols
2.5 Continuous beds or monoliths in CEC
2.6 Open tubular capillaries
2.7 Conclusions and prognostications
References

3. The Mobile Phase
3.1 Bubble prevention
3.2 Effect of organic solvents
References

4. Instrumentation
4.1 General instrumentation
4.2 Capillary columns
4.3 Detection
4.4 Microchips
4.5 Future developments
References

5. Applications for Small Molecules
5.1 Biomolecules and biopharmaceuticals
5.2 Pharmaceuticals and related analytes
5.3 Drugs of abuse
5.4 Ion analysis
5.5 Amino acids
5.6 Enantiomeric separations
5.7 Conclusions
References

6. Applications for Biopolymers
6.1 Potential of CEC
6.2 Stationary phase and packing considerations
6.3 Carbohydrates
6.4 Peptides, proteins, and antibodies
6.5 Nucleic acids and oligonucleotides
6.6 Biopolymer adsorption and interaction
6.7 Conclusions
References

7. Method Transfer from HPLC
7.1 Differences Between CEC and PEC in Method Transfer from HPLC
7.2 Comparison of Basic requirements in CEC and HPLC
7.3 Packings and stationary phases in CEC
7.4 Mobile phases and buffers in CEC
7.5 Sample preparation requirements
7.6 Isocratic, step-gradient, and true gradient conditions
7.7 Detector conditions
7.8 Voltage conditions
References
Further reading

8. Method Development and Optimization
8.1 Analytical method requirements
8.2 Analyte standard characterization
8.3 Literature search, background information, and prior art
8.4 Adaptability and choice of possible methods
8.5 Instrumentation preparation and initial studies
8.6 Sample and method optimization
8.7 Demonstration of analytical figures of merit with standards and system suitability samples
8.8 Evaluation with actual samples
References
Further reading

9. Conclusions and Future Developments
9.1 Applications as the driving force for CEC
9.2 Analysis of complex samples by CEC
9.3 Specialized applications
9.4 The ideal capillary, liquid separations technique References

Glossary

Index
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  • Anonymous

    Posted May 12, 2000

    Much-needed introduction to CEC

    This is the first book I've seen to provide a good background and survey of the literature of CEC/PEC. Separation scientists who already have an extensive knowledge of CEC may not find a lot of new information here, but the book will be extremely helpful for those who want to learn more about the technology, including its advantages and disadvantages. While the book is extensively illustrated, I wouldn't have minded seeing some photos of CEC apparatus. A good index and detailed TOC make for easy, efficient searching of the text.

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