Determination of Trace Elements / Edition 1

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Very good 1 volume, please be aware of language, air mail shipment from Germany within 2-6 weeks, we deliver to any country-please ask us to enable delivery to your country! ... *****PLEASE NOTE: This item is shipping from an authorized seller in Europe. In the event that a return is necessary, you will be able to return your item within the US. To learn more about our European sellers and policies see the BookQuest FAQ section***** Read more Show Less

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Overview

This easy-to-use handbook guides the reader through the maze of trace element analysis. It highlights the advantages and disadvantages of individual techniques and enables the reader to select a judicious procedure for solving all kinds of analytical problems.
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Editorial Reviews

Booknews
A desk reference that describes all the main techniques for the quantitative determination of trace elements, including the advantages and disadvantages of each method, as written by specialists in each technique. The volume opens with four chapters that deal with general topics concerning all methods: systematic errors, quality control, sampling and preconcentration. The following seven chapters describe the main methods for trace element analysis. The last two chapters describe the application of the various methods in two areas, one dealing with speciation and the other with biological samples. Annotation c. Book News, Inc., Portland, OR (booknews.com)
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Product Details

  • ISBN-13: 9783527284245
  • Publisher: Wiley, John & Sons, Incorporated
  • Publication date: 10/17/1994
  • Edition number: 1
  • Pages: 608
  • Product dimensions: 6.95 (w) x 9.80 (h) x 1.29 (d)

Table of Contents

Systematic errors and their avoidance 4
Systematic errors during the analytical procedure 20
Basic rules for the recognition and elimination of systematic errors 29
Errors in analytical results 40
Accuracy 41
Measuring trace concentrations 42
The problem of detection 42
Practical applications 52
Reporting results at small concentrations 53
Changes in trace element composition 62
Pre-sampling considerations 77
Aspects of sampling 83
Sample decomposition 94
Separation and preconcentration of trace elements by coprecipitation 110
Separation and preconcentration of trace elements by flotation 114
Preconcentration and separation of trace elements by solvent extraction 118
Separation and preconcentration of trace elements by ion-exchange 128
Separation and preconcentration by sorption 137
Literature 147
Quality of results 148
Standards and chemicals 150
Sample preparation 152
Theory 154
Major components of the instrument 155
Radiation sources 156
Wavelength selection system 159
Atomization by flame 164
Instruments 172
Electrothermal atomization 173
Hydride generation 178
Interferences 180
Instrumental background corrections 183
Modifiers 187
Automation 188
Atomic spectrometry with plasma sources 192
Plasma sources and sampling 201
Plasma optical emission spectrometry 217
Plasma mass spectrometry 226
Basic nuclear physics 255
Gamma detection systems 267
Irradiation 278
Instrumental neutron activation analysis (INAA) 280
Samples dissolution 312
Radiochemical separations 316
General review of X-ray photoelectron and auger electron spectroscopies 362
XPS/AES applications in trace element determination 384
Anodic and cathodic stripping voltammetry 394
Non-stripping methods 405
Potentiometric stripping 405
Adsorptive stripping voltammetry 408
Analytical information from interfaced chromatography with specific element detection 427
Element-selective gas chromatographic detection 429
Classes of atomic plasma emission chromatographic detectors 434
The plasma-chromatograph interface 436
Analytical GC applications 438
Liquid chromatographic applications 448
Supercritical fluid chromatographic (SFC) applications 452
Chromatographic detection by plasma-mass spectrometry 453
Future directions for trace analysis 455
Principles of radiotracer methods 471
Spatial (surface) speciation by nuclear techniques 479
Phase speciation and the use of radioanalysis 493
Chemical speciation of trace elements 504
Need for trace element analysis of biomaterials 545
Biological standardization 549
Analytical standardization 556
Clinical specimens from human subjects 563
Environmental biomonitoring for toxicants 567
Biomineral imbalances and health effects 575
Trace elements and high altitude populations 577
Reference values for trace elements in human specimens 580
Reference parameters for data interpretation 586
The future 586
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