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Experimental Organometallic Chemistry: A Practicum in Synthesis and Characterization

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Overview

Offers the latest synthetic methodology and characterization techniques used in organometallic chemistry. Describes specialized techniques for difficult synthesis, as well as handling and sampling techniques used by leading experimentalists worldwide. Provides timely, useful information for any scientist who handles or characterizes organometallic compounds.
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Product Details

  • ISBN-13: 9780841214385
  • Publisher: American Chemical Society
  • Publication date: 11/28/1987
  • Series: ACS Symposium Series
  • Pages: 312
  • Product dimensions: 6.20 (w) x 9.10 (h) x 1.00 (d)

Meet the Author

AT&T Bell Laboratories

Texas A&M University

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Table of Contents

Techniques in Organometallic Chemistry Cannula Techniques HPLC Analysis Low-Temperature Chromatography Column IR Radiation as a Heat Source Techniques in the Handling of Highly Reduced Organometallics Preparation and Isolation of Crystalline Samples Recrystallization Apparatus Apparatus for UV Photochemical Reactions Distillation Flask for Use with a Heating Mantle Greaseless Stillheads Vacuum Line Techniques Assay of Ligand-Derived Gases Semiautomatic Gas Titration Device Multipurpose Vacuum Line Designs Greaseless Double Manifolds and Schlenkware Diverse Synthesis and Purification Procedures Facile and Inexpensive Repair of Drybox Gloves Continuous Inert Gas Purge Glovebox Cooling of Reactions Inside a Glovebox Using Metal Atoms and Molecular High-Temperature Species Heated Inlet System Recovering Air-Sensitive Products Versatile Sonochemical Reaction Vessels Pressure Reactors for Reactivity Studies Characterization of Inorganic and Organometallic Complexes Detection of Dihydrogen Complexes Method for Sealing and Opening NMR Tubes Method for Acquiring IR Spectral Data Simple Low-Temperature Solution IR Cell Quantum Yield Determination Spectrophotometric Cell Handling of Reactive Compounds for X-Ray Structure Analysis In Situ Crystal Growth Photoelectron Spectroscopy

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