Introduction to Microwave Sample Preparation: Theory and Practice

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Overview

Provides a theoretical basis for understanding microwave acid sampling requiring elemental or chemical analysis.
Describes techniques and equipment found most effective.
Gives direct practical applications of the methods to a variety of sample types. Covers most aspects of closed vessel microwave digestion and open vessel acid composition.
Demonstrates fundamental relationships that can be used to predict the conditions that will occur under specific parameter settings. Addresses safety considerations for each technique demonstrated. This book is truly multidisciplinary--its techniques can be used in inorganic elemental analysis, sample digestion, food analysis,
environmental sample preparation chemistry, and other areas.
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Product Details

  • ISBN-13: 9780841214507
  • Publisher: American Chemical Society
  • Publication date: 5/28/1988
  • Series: ACS Professional Reference Book Series
  • Pages: 288
  • Product dimensions: 6.10 (w) x 8.90 (h) x 1.00 (d)

Table of Contents

Introduction to Microwave Acid Decomposition Microwave Heating: Theoretical Concepts and Equipment Design Guidelines for Developing Microwave Dissolution Methods for Geological and Metallurgical Samples Open Reflux Vessels for Microwave Digestion: Botanical, Biological, and Food Samples for Elemental Analysis by Automated FIA/ICP Applications of Microwave Digestion in the Pharmaceutical Industry Monitoring and Predicting Temperature and Pressure in Microwave Dissolution Microwave Digestion of Biological Samples for Selenium Analysis by Electrothermal Atomic Absorption Spectrometry Kjeldahl Nitrogen Determination Using a Microwave System Remote Operation of Microwave Systems: for Solids Content Analysis and Chemical Dissolution in Highly Radioactive Environments Manual and Robotically Controlled Microwave Pressure Dissolution of Minerals Safety Guidelines for Microwave Systems in the Analytical Laboratory

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