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Mössbauer Spectroscopy in Materials Science / Edition 1

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Overview

This book is intended for those who are interested in practical applications of Mössbauer spectroscopy and therefore demands a basic knowledge of the underlying principles. The current state of the art is demonstrated using examples from materials science drawn from the following areas: Chemistry, mineralogy and metallurgy, artificially structured materials, nanosized materials and quasicrystals, and experimental techniques and data processing. The various techniques of Mössbauer spectroscopy are reviewed (transmission geometry, source experiments, detection of conversion electrons, backscattering geometry, various probe atoms, etc.). Studies of technologically important materials are presented (oxides, alloys, phosphates, fluorides, nitrides, steels, diamonds, minerals both terrestrial and extraterrestrial, zeolites, multilayers, amorphous solids, nanocrystalline alloys, etc.). Methodological aspects and new trends are illustrated using examples of experimental procedures comprising measurements in situ, under controlled atmosphere, at high pressure, with synchrotron radiation, as well as new instrumentation (including a miniaturised spectrometer for space missions) and data evaluation software.
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Product Details

  • ISBN-13: 9780792356400
  • Publisher: Springer Netherlands
  • Publication date: 9/5/2007
  • Series: Nato Science Partnership Subseries: 3 (closed) , #66
  • Edition description: 1999
  • Edition number: 1
  • Pages: 432
  • Product dimensions: 9.21 (w) x 6.14 (h) x 1.00 (d)

Table of Contents

Preface
Structure and Properties of Tin-Doped Metal Oxides1
The Kinetics of the Phase Transition in Ferrosilicon System13
Fluoride-Ion Conductors Derived from the Fluorite Type25
The Ba[subscript 1-x]Sn[subscript x]Cl[subscript 1+y]F[subscript 1-y] Solid Solution39
The Mechanism of [beta]-Fe[subscript 2]O[subscript 3] Formation by Solid-State Reaction between NaCl and Fe[subscript 2](SO[subscript 4])[subscript 3]49
Mossbauer Measurements of Solid Solutions (Fe[subscript x]Cr[subscript 1-x])[subscript 2]O[subscript 3], 057
Conversion Electron Mossbauer Spectroscopy63
[superscript 57]Fe Implanted in Diamond79
Iron States Following Cobalt Decay in Rutile Single Crystal87
Mossbauer Spectroscopy in Mineralogy and Geology97
High-Chromium Ferritic Steels107
Microstructural Analysis of Nuclear Reactor Pressure Vessel Steels119
Mechanomixing in Various Iron-Containing Binary Alloys131
Mossbauer Studies of Ball Milled Fe[subscript 1-x]S[subscript 1+x]143
Structural Evolution in Mechanically Alloyed Fe-Sn151
Mossbauer Investigation of Nitriding Processes161
Phase Composition of Steel Surfaces after Plasma Immersion Ion Implantation173
Spark Eroded Fe-N Powders183
Ion-Beam Irradiated Metallic Systems189
Electrodeposited, Ion Beam Mixed and Ball Milled FeCrNi Alloys203
Application of the Mossbauer Effect in Some Tribological Problems215
Mossbauer Studies in Magnetic Multilayers227
Mossbauer Spectrometry Applied to Iron-Based Nanocrystalline Alloys I243
Mossbauer Spectrometry Applied to Iron-Based Nanocrystalline Alloys II257
Radiation Damage of Nanocrystalline Materials273
Disordered Nanocrystalline Fe-Sn Alloys283
Iron Nanoparticles in X and Y Zeolites Prepared by Reduction with NaN[subscript 3]291
Quasielastic Mossbauer Scattering in Stable Icosahedral Al-Cu-Fe Quasicrystals299
Quasi-Elastic Processes Studied by Methods Sensitive to the Momentum and Energy Transfer307
Synchrotron Mossbauer Reflectometry in Materials Science323
Site Preference of [superscript 57]Co in Fe-Si Alloys after Grain Boundary Diffusion337
High Pressure Mossbauer Spectroscopy349
The Challenge of an Automatic Mossbauer Analysis359
Evaluation of Experimental Data: Lineshape and Goodness of Fit373
Confit for Windows 95385
YAP-Ce Scintillation Detector for Transmission Mossbauer Spectroscopy391
The Mossbauer Spectrometer as a Virtual Instrument399
Calibration of the Mossbauer Spectrometer Velocity by Optical Methods407
The Miniaturized Spectrometer MIMOS II413
Author Index427
Subject Index429
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