Macroscale and Microscale Organic Experiments / Edition 5

Hardcover (Print)
Rent
Rent from BN.com
$52.64
(Save 83%)
Est. Return Date: 11/22/2014
Used and New from Other Sellers
Used and New from Other Sellers
from $44.89
Usually ships in 1-2 business days
(Save 85%)
Other sellers (Hardcover)
  • All (12) from $44.89   
  • New (4) from $89.99   
  • Used (8) from $44.89   
Close
Sort by
Page 1 of 1
Showing All
Note: Marketplace items are not eligible for any BN.com coupons and promotions
$89.99
Seller since 2014

Feedback rating:

(179)

Condition:

New — never opened or used in original packaging.

Like New — packaging may have been opened. A "Like New" item is suitable to give as a gift.

Very Good — may have minor signs of wear on packaging but item works perfectly and has no damage.

Good — item is in good condition but packaging may have signs of shelf wear/aging or torn packaging. All specific defects should be noted in the Comments section associated with each item.

Acceptable — item is in working order but may show signs of wear such as scratches or torn packaging. All specific defects should be noted in the Comments section associated with each item.

Used — An item that has been opened and may show signs of wear. All specific defects should be noted in the Comments section associated with each item.

Refurbished — A used item that has been renewed or updated and verified to be in proper working condition. Not necessarily completed by the original manufacturer.

New
New

Ships from: acton, MA

Usually ships in 1-2 business days

  • Standard, 48 States
  • Standard (AK, HI)
$121.62
Seller since 2010

Feedback rating:

(55)

Condition: New
"New, ships through UPS and DHL. Excellent customer service. Satisfaction guaranteed!! "

Ships from: STERLING HEIGHTS, MI

Usually ships in 1-2 business days

  • Canadian
  • International
  • Standard, 48 States
  • Standard (AK, HI)
$129.95
Seller since 2014

Feedback rating:

(179)

Condition: New
New

Ships from: acton, MA

Usually ships in 1-2 business days

  • Standard, 48 States
  • Standard (AK, HI)
$146.91
Seller since 2014

Feedback rating:

(0)

Condition: New
Hardcover New in new dust jacket. Brand New US edition, 3-5 days shipping!

Ships from: Sausalito, CA

Usually ships in 1-2 business days

  • Canadian
  • International
  • Standard, 48 States
  • Standard (AK, HI)
  • Express, 48 States
  • Express (AK, HI)
Page 1 of 1
Showing All
Close
Sort by

Overview

The market leader for the full-year organic laboratory, this manual derives many experiments and procedures from the classic Feiser lab text, giving it an unsurpassed reputation for solid, authoritative content. The book includes new experiments that stress greener chemistry, updated NMR spectra, and a Premium Website that includes glassware-specific videos with pre-lab exercises. Offering a flexible mix of macroscale and microscale options for most experiments, this proven manual allows users to save on the purchase and disposal of expensive, sometimes hazardous organic chemicals. Macroscale versions can be used for less costly experiments, giving readers experience working with conventionally sized glassware.

Read More Show Less

Product Details

  • ISBN-13: 9780618590674
  • Publisher: Cengage Learning
  • Publication date: 3/2/2006
  • Edition description: 5TH
  • Edition number: 5
  • Pages: 880
  • Product dimensions: 7.70 (w) x 9.30 (h) x 1.50 (d)

Meet the Author


Ken Williamson is retired from Mt. Holyoke College where he taught the organic chemistry laboratory course. He is an established authority on microscale techniques and regularly holds workshops and travels to campuses in the U.S., Canada, and Europe to demonstrate the use of microscale.

A PhD from Pennsylvania State University, Katherine Masters is director of the organic chemistry laboratory courses at Penn State.

Read More Show Less

Table of Contents

1. Introduction. 2. Laboratory Safety, Courtesy, and Waste Disposal Techniques. 3. Melting Points and Boiling Points. 4. Recrystallization. 5. Distillation. 6. Steam Distillation, Vacuum Distillation, and Sublimation. 7. Extraction. 8. Thin-Layer Chromatography: Analysis of Analgesics and Isolating Lycopene from Tomato Paste. 9. Column Chromatography: Fluorenone, Cholesteryl Acetate, Acetylferrocene, and Plant Pigments. 10. Gas Chromatography: Analysis of Alkene Isomers. 11. Infrared Spectroscopy. 12. Nuclear Magnetic Resonance Spectroscopy. 13. Mass Spectroscopy. 14. Ultraviolet Spectroscopy, Refractive Indices, and Qualitative Instrumental Organic Analysis. 15. Computational Chemistry Elimination, Substitution, and Addition. 16. The SN2 Reaction: 1-Bromobutane. 17. Nucleophilic Substitution Reactions of Alkyl Halides. 18. Radical Initiated Chlorination of 1-Chlorobutane. 19. Alkenes from Alcohols: Cyclohexene from Cyclohexanol. 20. Bromination and Debromination: Purification of Cholesterol. 21. Dichlorocarbene Oxidation and Reduction. 22. Oxidation: Cyclohexanol to Cyclohexanone; Cyclohexanone to Adipic Acid. 23. The Cannizzaro Reaction: Simultaneous Synthesis of an Alcohol and an Acid in the Absence of Solvent. 24. Oxidative Coupling of Alkynes: 2,7-Dimethyl-3,5-octadiyn-2,7-diol. 25. Catalytic Hydrogenation. 26. Sodium Borohydride Reduction of 2-Methylcyclohexanone: A Problem in Conformational Analysis. 27. Epoxidation of Cholesterol. Aromatic Substitution and Elimination. 28. Nitration of Methyl Benzoate 29. Friedel-Crafts Alkylation of Benzene and Dimethoxybenzene; Host-Guest Chemistry. 30. Alkylation of Mesitylene. 31. The Friedel-Crafts Reaction: Anthraquinone and Anthracene. 32. Friedel-Crafts Acylation of Ferrocene: Acetylferrocene. 33. Reactions of Triphenylmethyl Carbocation, Carbanion, and Radical. 34. 1,2,3,4-Tetraphenylnaphthalene via Benzyne. 35. Triptycene via Benzyne Reactions of Aldehydes and Ketones. 36. Aldehydes and Ketones. 37. Dibenzalacetone by the Aldol Condensation. 38. Grignard Synthesis of Triphenylmethanol and Benzoic Acid. 39. The Wittig and Wittig-Horner Reactions Reactions of Carboxylic Acids, Esters, and Amines. 40. Esterification and Hydrolysis. 41. Acetylsalicylic Acid (Aspirin). 42. Malonic Ester of a Barbiturate. 43. Amines. 44. The Sandmeyer Reaction: 1-Bromo-4-chlorobenzene, 2-Iodobenzoic Acid, and 4-Chlorotoluene. 45. Synthesis and Bioessay of Sulfanilamide and Derivatives. 46. Dyes and Dyeing. 47. Martius Yellow. 48. Diels-Alder Reaction. 49. Ferrocene [Bis(cyclopentadienyl)iron]. 50. A Diels-Alder Reaction Puzzle: The Reaction of 2,4-Hexadien-1-ol with Maleic Anhydride. 51. Tetraphenylcyclopentadienone. 52. Hexaphenylbenzene and Dimethyl Tetraphenylphthalate. Derivatives of 1,2-Diphenylethane: A Multistep Synthesis. 53. The Benzoin Condensation: Catalysis by the Cyanide Ion and Thiamine. 54. Nitric Acid Oxidation; Preparation of Benzil from Benzoin; and Synthesis of a Heterocycle: Diphenylquinoxaline. 55. Borohydride Reduction of a Ketone: Hydrobenzoin from Benzil. 56. The Synthesis of 2,2-Dimethyl-1,5-dioxolane; The Acetonide Derivative of a Vicinal Diol. 57. The 1,4-Addition: Reductive Acetylation of Benzil. 58. Synthesis of an Alkyne from an Alkene; Bromination and Dehydrobromination: Stilbene and Diphenylacetylene. 59. The Perkin Reaction: Synthesis of a-Phenylcinnamic Acid. 60. Multicomponent Reactions: The Aqueous Passerini Reaction. 61. Chemiluminescence: Syntheses of Cyalume and Luminol. 62. Photochemistry: The Synthesis of Benzopinacol Natural Product Chemistry and Biochemistry. 63. Carbohydrates and Sweeteners. 64. Virstatin, a Possible Treatment for Cholera. 65. Biosynthesis of Ethanol and Enzymatic Reactions. 66. The Synthesis of Natural Products: Pseudopellitierene and Camphor. 67. Polymers: Synthesis and Recycling. 68. Searching the Chemical Literature.

Read More Show Less

Customer Reviews

Be the first to write a review
( 0 )
Rating Distribution

5 Star

(0)

4 Star

(0)

3 Star

(0)

2 Star

(0)

1 Star

(0)

Your Rating:

Your Name: Create a Pen Name or

Barnes & Noble.com Review Rules

Our reader reviews allow you to share your comments on titles you liked, or didn't, with others. By submitting an online review, you are representing to Barnes & Noble.com that all information contained in your review is original and accurate in all respects, and that the submission of such content by you and the posting of such content by Barnes & Noble.com does not and will not violate the rights of any third party. Please follow the rules below to help ensure that your review can be posted.

Reviews by Our Customers Under the Age of 13

We highly value and respect everyone's opinion concerning the titles we offer. However, we cannot allow persons under the age of 13 to have accounts at BN.com or to post customer reviews. Please see our Terms of Use for more details.

What to exclude from your review:

Please do not write about reviews, commentary, or information posted on the product page. If you see any errors in the information on the product page, please send us an email.

Reviews should not contain any of the following:

  • - HTML tags, profanity, obscenities, vulgarities, or comments that defame anyone
  • - Time-sensitive information such as tour dates, signings, lectures, etc.
  • - Single-word reviews. Other people will read your review to discover why you liked or didn't like the title. Be descriptive.
  • - Comments focusing on the author or that may ruin the ending for others
  • - Phone numbers, addresses, URLs
  • - Pricing and availability information or alternative ordering information
  • - Advertisements or commercial solicitation

Reminder:

  • - By submitting a review, you grant to Barnes & Noble.com and its sublicensees the royalty-free, perpetual, irrevocable right and license to use the review in accordance with the Barnes & Noble.com Terms of Use.
  • - Barnes & Noble.com reserves the right not to post any review -- particularly those that do not follow the terms and conditions of these Rules. Barnes & Noble.com also reserves the right to remove any review at any time without notice.
  • - See Terms of Use for other conditions and disclaimers.
Search for Products You'd Like to Recommend

Recommend other products that relate to your review. Just search for them below and share!

Create a Pen Name

Your Pen Name is your unique identity on BN.com. It will appear on the reviews you write and other website activities. Your Pen Name cannot be edited, changed or deleted once submitted.

 
Your Pen Name can be any combination of alphanumeric characters (plus - and _), and must be at least two characters long.

Continue Anonymously

    If you find inappropriate content, please report it to Barnes & Noble
    Why is this product inappropriate?
    Comments (optional)