Materials Syntheses: A Practical Guide / Edition 1

Materials Syntheses: A Practical Guide / Edition 1

by Ulrich Schubert
     
 

Materials syntheses are generally more complex than syntheses of inorganic or organic compounds and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. It collects a

See more details below

Overview

Materials syntheses are generally more complex than syntheses of inorganic or organic compounds and specific characterization methods play a more important role. Materials synthesis protocols often suffer from unclarities, irreproducibility, lack in detail and lack in standards. The need to change this situation is the main motivation for this book. It collects a number of detailed protocols, ranging from organic polymers to carbonaceous and ceramic materials, from gels to porous and layered materials and from powders and nanoparticles to films. Preparation methods include intercalation and flux methods, sol-gel processing, templating methods for porous materials, sonochemistry or spray pyrolysis. Each contribution provides detailed and unambiguous descriptions of the hardware, specific characteristics of the procedure, scope of applicability as well as methods that unequivocally identify and characterize the material and allow checking whether the synthesis was successful. Written for: Researchers and graduate students in inorganic, organic, physical organic chemistry as well as material sciences studies

Read More

Product Details

ISBN-13:
9783211751244
Publisher:
Springer Vienna
Publication date:
07/19/2008
Edition description:
2008
Pages:
228
Product dimensions:
6.20(w) x 9.40(h) x 0.80(d)

Table of Contents

Preface 1

List of Contributors 3

Controlling Size and Morphology of Zeolite L 9

Zeolite A and ZK-4 21

Mesostructured Silica Thin Films 29

Organically Modified Monolithic Silica Aerogels 39

Porous Silica Gel by Acid Leaching of Metakaolin 47

Zirconia-Pillared Clays 53

Montmorillonites with Mixed Aluminum-Lanthanide Oxide Pillars 59

Birnessite-type Manganese Oxide by Redox Precipitation 65

Templated Carbon from Pyrolysis of Pyrene in Pillared Clay Matrices 71

Fiberous Carbon from Sepiolite Clay and Propylene 77

Aerosol Spray Synthesis of Porous Molybdenum Sulfide Powder 83

Sonochemically Prepared Molybdenum Sulfide 89

Doped Manganites 95

Lithium Manganese Oxide Prepared by Flux Methods 103

Nanoscale Magnesium Oxide 111

Nanostructured Pt-doped Tin Oxide Films 117

Organically Functionalized Silica Nanoparticles 127

Copper Nanoparticles in Silica 135

Copper Nanocrystals 143

Assembly of TOPO-Capped Silver NanoparticIes to Multilayered Films 149

Colloidal Dispersion of Gold NanoparticIes 155

One-dimensional Nanorods and Nanowires 163

Monolithic Tin-doped Silica Glass 169

Octaphenyloctasilsesquioxane and Polyphenylsilsesquioxane for Nanocomposites 179

Polysilsesquicarbodiimide Xerogels 193

Polyaniline - A Conducting Polymer 199

Allyl- and Hydroxytelechelic Poly(isobutylenes) 209

Symmetrically and Unsymmetrically Substituted Phthalocyanines 217

Index 227

Read More

Customer Reviews

Average Review:

Write a Review

and post it to your social network

     

Most Helpful Customer Reviews

See all customer reviews >