The Organic Chem Lab Survival Manual: A Student's Guide to Techniques / Edition 9

The Organic Chem Lab Survival Manual: A Student's Guide to Techniques / Edition 9

by James W. Zubrick
ISBN-10:
1118083393
ISBN-13:
9781118083390
Pub. Date:
10/16/2012
Publisher:
Wiley
ISBN-10:
1118083393
ISBN-13:
9781118083390
Pub. Date:
10/16/2012
Publisher:
Wiley
The Organic Chem Lab Survival Manual: A Student's Guide to Techniques / Edition 9

The Organic Chem Lab Survival Manual: A Student's Guide to Techniques / Edition 9

by James W. Zubrick
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Overview

The fourth edition of this student-friendly lab manual presents the basic techniques of the organic chemistry laboratory, with an emphasis on doing the work correctly the first time. It is designed to quickly build student proficiency in experimental procedures. New additions include a focus on computer software and hardware and expanded coverage of microscale laboratory equipment to include microscale and ultramicroscale boiling point determination, flash chromatography using Pasteur pipets, and Keck clips used to keep your jointware setups together with possibly fewer clamps.

Product Details

ISBN-13: 9781118083390
Publisher: Wiley
Publication date: 10/16/2012
Edition description: Older Edition
Pages: 368
Product dimensions: 6.00(w) x 8.90(h) x 2.00(d)

About the Author

James W. Zubrick is the author of The Organic Chem Lab Survival Manual: A Student's Guide to Techniques, 10th Edition, published by Wiley.

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Table of Contents

Safety First, Last, and Always.
Keeping a Notebook.
Interpreting a Handbook.
Jointware.
Microscale Jointware.
Other Interesting Equipment.
Pipet Tips.
Syringes, Needles, and Septa.
Clean and Dry.
Drying Agents.
On Products.
The Melting Point Experiment.
Recrystallization.
Recrystallization: Microscale.
Extraction and Washing.
Extraction and Washing: Microscale.
And Now--Boiling Stones.
Sources of Heat.
Clamps and Clamping.
Distillation.
Microscale Distillation.
Reflux and Addition.
Reflux: Microscale.
Sublimation.
Microscale Boiling Point.
Chromatography: Some Generalities.
Thin-Layer Chromatography: TLC.
Wet-Column Chromatography.
Refractometry.
Instrumentation in the Lab.
Gas Chromatography.
HP Liquid Chromatography.
Infrared Spectroscopy.
Nuclear Magnetic Resonance (NMR).
Theory of Distillation.
Theory of Extraction.
Index.
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