Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach / Edition 2

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Overview

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, provides an introduction to the use of two-dimensional (2-D) nuclear magnetic resonance (NMR) spectroscopy to determine organic structure.
The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed.

• Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra
• Contains30 known and 30 unknown structure determination problems
• Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing.

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Editorial Reviews

From the Publisher
"I like [the book] a lot. Books that cover theory in depth AND lots of problems are (surprisingly) rare."--Steven M. Graham, St. John's University

"The abundance of problems and highly detailed glossary are especially noteworthy; the quality of the spectrum presentations is excellent [...] Overall organization works well, and the layout and other 'production values' are what one has long come to expect from [Academic Press]."--Barry Shapiro

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Product Details

  • ISBN-13: 9780123849700
  • Publisher: Elsevier Science
  • Publication date: 1/13/2012
  • Edition description: New Edition
  • Edition number: 2
  • Pages: 540
  • Product dimensions: 7.30 (w) x 9.00 (h) x 1.30 (d)

Table of Contents

PART I: Background and Methods Chapter 1: Introduction Chapter 2: Instrumental Considerations Chapter 3: Data Collection, Processing, and Plotting Chapter 4: 1H and 13C Chemical Shifts Chapter 5: Symmetry and Topicity Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling Chapter 7: Through-Space Effects: the Nuclear Overhauser Effect (NOE) Chapter 8: Molecular Dynamics Chapter 9: Strategies for Assigning Molecules Chapter 10: Strategies for Elucidating Unknown Molecular Structures PART II: Problems Chapter 11 Simple Assignment Problems Chapter 12: Complex Assignment Problems Chapter 13: Simple Unknown Problems Chapter 14: Complex Unknown Problems Chapter 15: NMR Resonance Assignment Problems Chapter 16: NMR Unknown Problems

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