Organocopper Reagents: A Practical Approach

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Overview

This essential laboratory handbook dispels the mystery surrounding organocopper compounds and offers expert guidance on how to overcome the many problems associated with their use. Authored by leading researchers, the book features clear, practical descriptions of key procedures used in the preparation and application of these highly specific reagents. In addition, the book contains a succinct historical overview of the field's development. Beginning and established researchers alike will find Organocopper Reagents: A Practical Approach an invaluable source of information on an exciting, fast-growing field.

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Editorial Reviews

Booknews
A laboratory manual detailing the procedures for the preparation and application of a group of highly specific reagents, and how to overcome the many problems associated with their use. Also includes a historical overview of organocopper chemistry; a description of starting material purification; and guidelines to the reaction, which are usually characterized by a high chemo-, regio-, and stereoselectivity. Begins a series providing practical and accessible laboratory guides for new and experienced researchers unfamiliar with the particular area. Annotation c. Book News, Inc., Portland, OR (booknews.com)
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Product Details

  • ISBN-13: 9780198557586
  • Publisher: Oxford University Press, USA
  • Publication date: 5/18/1995
  • Series: Practical Approach in Chemistry Series
  • Format: Spiral Bound
  • Pages: 376
  • Product dimensions: 6.75 (w) x 9.25 (h) x 1.05 (d)

Table of Contents

List of contributors
Abbreviations
1 Organocopper chemistry: an overview 1
2 General procedures: starting materials and reaction guidelines 27
3 Preparation of organocopper reagents using active copper 73
4 Preparation of highly functionalized reagents 85
5 Higher order cyanocuprates 105
6 Me[subscript 3]SiCl-accelerated conjugate addition reactions of organocopper reagents 129
7 Boron trifluoride/aluminium trichloride-mediated conjugate addition and substitution reactions 143
8 Asymmetric conjugate addition 159
9 Conjugate addition - enolate-trapping reactions 185
10 The Sonogashira Cu-Pd-catalysed alkyne coupling reaction 217
11 Alkyne carbocupration and polyene synthesis 237
12 Synthetic applications of silylcuprates and stannylcuprates 257
13 Mechanistic studies of organocopper reactions 293
Appendix 1: Compilation of organocopper preparations 307
Appendix 2: List of suppliers 353
Index 357
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