Pitfalls and Errors of HPLC in Pictures / Edition 1

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Overview

Adding 13 examples to this new, third edition, Veronika Meyer now offers solutions for nearly 100 problems. All the examples are accompanied by a concise, instructive text and an informative figure, including essential fundamentals as well as such helpful strategies as equipment tests or quality assurance strategies. A practice-oriented aid to obtaining correct and reliable analytical results.

From the reviews of a previous edition:
'This is a giant of a little book on HPLC.'
(Analytical Chemistry)

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Product Details

  • ISBN-13: 9783527313723
  • Publisher: Wiley
  • Publication date: 4/28/2006
  • Edition description: 2nd, Revised and Enlarged Edition
  • Edition number: 1
  • Pages: 199
  • Product dimensions: 6.79 (w) x 9.57 (h) x 0.41 (d)

Meet the Author

Following an apprenticeship as laboratory assistant, Veronika R. Meyer studied chemistry at the university of applied sciences in Burgdorf (Switzerland). From 1976 to 1998 she worked with HPLC at Berne University, where she also completed her PhD thesis in Chemistry. Afterwards she spent her post-doc time at the Weizmann-Institute in Rehovot (Israel) and at the University of Delaware, Newark, DE. Since 1998 she is working for EMPA (Swiss Federal Laboratories for Materials Testing and Research) in St. Gallen. The fist German edition of her textbook "Practical High-Performance Liquid Chromatography" was published in 1979. Veronika R. Meyer is author of numerous papers in international journals and teaches at Berne University.

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Table of Contents

INTRODUCTION
FUNDAMENTALS
New: The playground presented as an Ishikawa diagram
PITFALLS AND SOURCES OF ERROR
New: Inadequate purity of a mobile phase solvent
New: Decomposition by the sample vial
New: Artifact peaks from the vial septum
New: Recovery and peak shape problems with proteins
New: Thermal non-equilibrium within the column
New: Integration threshold and number of detected peaks
New: Detector time constant and peak shape
USEFUL STRATEGIES
New: A linearity test
New: Some elements of validation
New: A validation example
New: Measurement uncertainty
New: Formal quality assurance systems

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