Temperature-Programmed Reduction For Solid Materials Characterization

Temperature-Programmed Reduction For Solid Materials Characterization

by Alan Jones, Brian D. McNicol
     
 

ISBN-10: 082477583X

ISBN-13: 9780824775834

Pub. Date: 05/01/1986

Publisher: Taylor & Francis

The only current, comprehensive book of its kind, this single-source reference brings together all the work to date on Temperature-Programmed Reduction (TPR), a relatively new technique -- involving low capital investment -- that facilitates fast and easy access to information about the precise condition of species present in and on solids. Temperature-Programmed…  See more details below

Overview

The only current, comprehensive book of its kind, this single-source reference brings together all the work to date on Temperature-Programmed Reduction (TPR), a relatively new technique -- involving low capital investment -- that facilitates fast and easy access to information about the precise condition of species present in and on solids. Temperature-Programmed Reduction for Solid Materials Characterization provides details of practical approaches in the use of TPR ... diagrams of both equipment and results produced ... descriptions of the parametric sensitivity of TPR and instrumentation used for its measurement ... up-to-date accounts of theory, practice, and published work on TPR ... various applications in numerous scientific fields, especially the characterization of catalysts ... and discussions of developing trends and future directions in temperature programming. Temperature-Programmed Reduction for Solid Materials Characterization serves as an indispensable sourcebook for chemical, industrial process, and petrochemical engineers; analytical, polymer, and materials chemists; metallurgists; and students in undergraduate- and graduate-level courses concerned with materials characterization, such as physical chemistry, analytical science, and materials science.

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Product Details

ISBN-13:
9780824775834
Publisher:
Taylor & Francis
Publication date:
05/01/1986
Series:
Chemical Industries Series, #24
Pages:
208
Product dimensions:
6.40(w) x 9.30(h) x 0.80(d)

Table of Contents

Prefaceiii
1.Introduction1
IBackground
IIApplications
References
2.Theoretical Aspects11
IThermodynamics
IIKinetics and Mechanisms of Reduction
IIIDerivation of Kinetic Parameters
IVEffects of Variation of Experimental Parameters
References
3.Experimental Methods and Instrumentation67
IGeneral Procedure
IIThermal Conductivity Detectors
IIIDetection by Pressure Changes of the Reacting Gas
IVDetection by Weight Changes of the Reducing Solid
VOther Methods
VIFurnace Design
VIIAutomated Apparatus for Measuring Temperature-Programmed Reduction, Desorption, and Oxidation
VIIIPractical Considerations
IXConclusions
References
4.Applications81
IZeolites
IIBulk Monometallic Materials
IIIBulk Bimetallic Materials
IVSupported Monometallic Materials
VSupported Bimetallic Materials
VIConclusions
References
5.Trends in Temperature Programming for Solid Characterization187
ICurrent Applications
IIFuture Applications
References
Index193

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