The New Edition of the Well-Regarded Handbook on GasChromatography
Since the publication of the highly successful first edition ofBasic Gas Chromatography, the practice of chromatography hasundergone several notable developments. Basic GasChromatography, Second Edition covers the latest in the field,giving readers the most up-to-date guide available, whilemaintaining the first edition's practical, applied approach to thesubject and its accessibility to a wide range of readers.
The text provides comprehensive coverage of basic topics in thefield, such as stationary phases, packed columns and inlets,capillary columns and inlets, detectors, and qualitative andquantitative analysis. At the same time, the coverage also featureskey additions and updated topics including:
- Gas chromatography-mass spectrometry (GC-MS)
- Sampling methods
- Multidimensional gas chromatography
- Fast gas chromatography
- Gas chromatography analysis of nonvolatile compounds
- Inverse gas chromatography and pyrolysis gaschromatography
Along with these new and updated topics, the references,resources, and Web sites in Basic Gas Chromatography have beenrevised to reflect the state of the field. Concise and fundamentalin its coverage, Basic Gas Chromatography, Second Editionremains the standard handbook for everyone from undergraduatesstudying analytical chemistry to working industrial chemists.
About the Author
Harold M. Mcnair, PhD, known internationally as a leadingresearcher and educator in the field of chromatography, iscurrently Professor Emeritus of Chemistry at Virginia Tech.
James M. Miller, PhD, is Professor Emeritus of Chemistryat Drew University, where he taught for thirty-six years. He isalso the author of Chromatography: Concepts and Contrasts(Wiley).
Table of Contents
PREFACE TO THE SECOND EDITION.
A Brief History.
Overview: Advantages and Disadvantages.
2 INSTRUMENT OVERVIEW.
Flow Control and Measurement.
Sample Inlets and Sampling Devices.
3 BASIC CONCEPTS AND TERMS.
Definitions, Terms, and Symbols.
The Rate Theory.
A Redefinition of H.
The Achievement of Separation.
4 STATIONARY PHASES.
Selecting a Column.
Classification of Stationary Phases for GLC.
Liquid Stationary Phases (GLC).
Solid Stationary Phases (GSC).
5 PACKED COLUMNS AND INLETS.
Liquid Stationary Phases.
Solid Stationary Phases (GSC).
Analysis of Other Inorganics.
Inlets for Liquid Samples and Solutions.
Upgrading for Capillary Columns.
6 CAPILLARY COLUMNS AND INLETS.
Types of OT Columns.
OT Column Tubing.
Advantages of OT Columns.
Capillary Inlet Systems.
Classification of Detectors.
Flame Ionization Detector (FID).
Thermal Conductivity Detector (TCD).
Electron Capture Detector (ECD).
8 QUALITATIVE AND QUANTITATIVE ANALYSIS.
9 PROGRAMMED TEMPERATURE.
Advantages and Disadvantages of PTGC.
Requirements of PTGC.
Theory of PTGC.
10 GAS CHROMATOGRAPHY–MASS SPECTROMETRY(GC–MS).
Limitations of GC–MS Systems.
11 MULTIDIMENSIONAL GAS CHROMATOGRAPHY.
Fundamental Principles of Multidimensional Chromatography.
GC×GC with Heart Cutting.
LC×GC with Heart Cutting.
12 SAMPLING METHODS.
Liquid–Liquid Extraction (LLE).
Solid–Liquid Extraction: Soxhlet Extraction andAccelerated Solvent Extraction (ASE).
Liquid–Solid Extraction: Solid-Phase Extraction (SPE).
Liquid- or Solid-Vapor Extraction: Headspace Extraction.
Solid-Phase Micro-extraction (SPME).
Additional Techniques and Summary.
13 SPECIAL TOPICS.
Chiral Analysis by GC.
GC Analysis of Nonvolatile Compounds.
14 TROUBLESHOOTING GC SYSTEMS.
APPENDIX I SYMBOLS AND ACRONYMS.
APPENDIX II GUIDELINES FOR SELECTING CAPILLARY COLUMNS.
APPENDIX III GC: HOW TO AVOID PROBLEMS.
APPENDIX IV CALCULATION OF SPLIT RATIO FOR SPLIT INJECTION ON OTCOLUMNS.
APPENDIX V OPERATING CONDITIONS FOR CAPILLARY COLUMNS.
APPENDIX VI OV LIQUID PHASES PHYSICAL PROPERTY DATA.
APPENDIX VII SOME COMPRESSIBILITY CORRECTION FACTORS (J).
APPENDIX VIII SOME INTERNET WEBSITES FOR GASCHROMATOGRAPHERS.
APPENDIX IX OTHER BOOKS ON GAS CHROMATOGRAPHY.
INDEX OF APPLICATIONS.
What People are Saying About This
"The book should appeal to readers with varying levels of education and emphasises a practical, applied approach to the subject. Basic Gas Chromatography, 2nd Edition remains the standard handbook for everyone from undergraduates studying analytical chemistry to working industrial chemists. It is particularly suited for intensive short courses." (Chemistry Journals, 11 April 2011)