Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach / Edition 2

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach / Edition 2

by Jeffrey H. Simpson
ISBN-10:
0123849705
ISBN-13:
9780123849700
Pub. Date:
01/13/2012
Publisher:
Elsevier Science
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Overview

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach / Edition 2

Organic Structure Determination Using 2-D NMR Spectroscopy: A Problem-Based Approach, Second Edition, is a primary text for a course in two-dimensional (2-D) nuclear magnetic resonance (NMR) techniques, with the goal to learn to identify organic molecular structure. It presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra.

The book begins with a discussion of the NMR technique, while subsequent chapters cover instrumental considerations; data collection, processing, and plotting; chemical shifts; symmetry and topicity; through-bond effects; and through-space effects. The book also covers molecular dynamics; strategies for assigning resonances to atoms within a molecule; strategies for elucidating unknown molecular structures; simple and complex assignment problems; and simple and complex unknown problems. Each chapter includes problems that will enable readers to test their understanding of the material discussed. The book contains 30 known and 30 unknown structure determination problems. It also features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing.

This book will stand as a single source to which instructors and students can go to obtain a comprehensive compendium of NMR problems of varying difficulty.

  • Presents strategies for assigning resonances to known structures and for deducing structures of unknown organic molecules based on their NMR spectra
  • Contains 30 known and 30 unknown structure determination problems
  • Features a supporting website from which instructors can download the structures of the unknowns in selected chapters, digital versions of all figures, and raw data sets for processing

Product Details

ISBN-13: 9780123849700
Publisher: Elsevier Science
Publication date: 01/13/2012
Edition description: New Edition
Pages: 540
Product dimensions: 7.30(w) x 9.00(h) x 1.30(d)

Table of Contents

PART I: Background and Methods Chapter 1: Introduction Chapter 2: Instrumental Considerations Chapter 3: Data Collection, Processing, and Plotting Chapter 4: 1H and 13C Chemical Shifts Chapter 5: Symmetry and Topicity Chapter 6: Through-Bond Effects: Spin-Spin (J) Coupling Chapter 7: Through-Space Effects: the Nuclear Overhauser Effect (NOE) Chapter 8: Molecular Dynamics Chapter 9: Strategies for Assigning Molecules Chapter 10: Strategies for Elucidating Unknown Molecular Structures PART II: Problems Chapter 11 Simple Assignment Problems Chapter 12: Complex Assignment Problems Chapter 13: Simple Unknown Problems Chapter 14: Complex Unknown Problems Chapter 15: NMR Resonance Assignment Problems Chapter 16: NMR Unknown Problems

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