Structure Elucidation by Modern NMR: A Workbook

by Helmut Duddeck, Wolfgang Dietrich, Gabor Toth

Overview

During the last few years, routine applications of NMR techniques have been further developed. Spectrometers of the latest generation offer new types of experiments, such as spinlock and inverse-detected methods. In this third, revised and expanded edition, new methodology is introduced and incorporated into new exercises. In addition, a new chapter has been introduced which demonstrates the fully detailed interpretation of two typical examples.

Product Details

ISBN-13:	9783798511118
Publisher:	Springer-Verlag New York, LLC
Publication date:	07/10/1998
Edition description:	Third Edition 1998
Pages:	211
Product dimensions:	6.10(w) x 9.25(h) x 0.02(d)

Table of Contents

Introduction.- Methodology.- High Magnetic Fields. One-dimensional 1H,1H Correlation. Two-Dimensional 1H,13C One-Bond Correlation. Two-Dimensional 1H,13C Long-Range Correlation. NOE Experiments. 13C,13C-Correlation.- Two Demonstration Examples. Rearrangement of a Benzothiazepine to a Benzothiazole Derivative. Structure Elucidation of a Triterpene Saponin.- Exercises.- Strategies.- Solutions.